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What’s new in MDSolids 4.0.0:. MDSolids is a professional application oriented towards both teachers and students interested in the Mechanics .
Category:Engineering textbooksField of the Invention
The present invention relates generally to calibration of spectroscopic measurement systems. More specifically, the present invention relates to a calibration device and method for a tunable laser spectrometer.
Related Art
Inspections of ware in which a sample is placed within a sealed vessel (such as an inspected pipe) present a difficult calibration problem. In addition to the problem of ensuring that the measurements are accurate, the measurement system must be able to be calibrated when the spectrometer is applied to different types of measuring vessels.
The use of spectroscopic techniques, such as near-infrared, often pose difficult calibration problems because these types of measuring vessels can be opaque, containing gases or liquids, or containing a highly reflective material. Furthermore, the use of infrared beams can pose difficult problems with calibrations since it is difficult to obtain an accurate reference spectrum in the infrared range with the resulting measurements requiring precise temperature control.
The thermal conductivity of the material will, of course, affect the spectrum and, therefore, the calibration. In addition, the spectral excitation of the sample material will lead to a temperature shift in the material. The temperature shift leads to spectral distortion.
Current spectroscopic techniques for measuring sample material in an inspected pipe use a direct IR beam rather than a tunable laser beam. In the case of the former, the sample is heated by an external source and a portion of the beam is reflected from the material surface, whereas, in the case of a tunable laser, a portion of the beam is directed to a detector to measure the reflected beam that is scattered by the gas or liquid sample.
When measuring in a pipe, the calibration must account for the thermal conductivity and density of the
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